Thursday, April 29, 2010

THE LAB...

All right, everyone. I'm pretty sure everyone is pretty confused on what we are supposed to do for THE LAB, so I'm going to try and put out there what I think we are supposed to do. Scully, I'm counting on you especially to call me out for being wrong on anything.

Ok, I'll start off with some definitons:

  1. titration-adding NaOH to KHP until it turns a "the lightest shade of pink"
  2. KHP-potassium hydrogen phthalate; it's the stuff that look like big salt
  3. NaOH-sodium hydroxide; it's what goes in the buret, and is located in a keg-thing by the microwaves
  4. phenolphthalein-[fee-nawl-thal-een] stuff that is in X-lax (not the lacrosse possition!) it's what makes the titration, your mixture of NaOH and KHP turn pink

Next off, some general starter. I'll leave some stuff some other guys to comment though

  1. --get 2, TWO, samples of KHP; keep it as close as you can to 0.50 g, but it's better to go lower
  2. --dissolve KHP in a beaker of ionized water and 2, TWO, drops of pheolthinggummy; swirl it around until it is completely dissolved
  3. --while one guy is doing step two, the other can use the tiny beaker Dr. B gave us, fill it with NaOH from the keg-thing, and pour it into the buret.
  4. initial NaOH volume reading=0.something(measure from zero); record this before you titrate;
  5. stick the beaker of dissolved KHP under the buret and open the valve. THIS IS YOU TITRATING
  6. When you're titrating, let in 5 or so mL of NaOH, then swirl, let in another 5 and swirl, let in another 5 and swirl, AND THEN start adding it in drops sssslllooooowwlllllyyyyyyyy (you add it slowly because the point where it is "the faintest shade of pink" arrives really fast)
  7. after you titrate, make your Final NaOH volume reading
  8. Final NaOH volume reading= somewhere in the teens(measure from zero)

Now all you do is repeat the steps, except you don't have to necessarily add more NaOH. You can just go from where the last one was. You just have to take that into account in your volume readings.

Ok, I really hoped that helped some of you. If it didn't, well I went to St. Ann, you can't expect me to be that good.

AND IF YOU THINK I'M WRONG, FREAKIN' TELL ME. INFALLIBLE IS NOT ME. that guy's German, and is probably just waking up right now to celebrate some Jesus in Rome. If he isn't somewhere else in the world, but I digress.

goodnight!

15 comments:

  1. Remember: When the red line on the buret knob is horizontal, the valve is closed. When it is vertical, the valve is open. Make sure to close the valve before putting anything into the buret.

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  2. I would like to take a moment to thank Mr. McCaffery for this. Kyle this actually cleared it up quite a bit for me.

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  3. nice blog kyle, i think dr b wants us to have 3 titrations a day so we might need to pick up the pace a bit, but this should be easier since we (might) understand the process now...

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  4. dont forget guys the key is to go SLOW
    also im bringing gloves for everyone tomorrow

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  5. and remember if you still need a little help, copy all of the procedure notes in the lab to your lab notebook

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  6. remember to not have any of the procedure hard copy notes in the presence of Dr. B while doing the lab.

    great blog kyle

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  7. Good practice for Titration:
    http://www.sciencegeek.net/Shockwave/Titration.htm

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  8. thanks for the blog kyle it really helped alot, and pay attention to the level of the burret when you doing the lab so you know at what level things go wrong

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  9. Dr.B told me that you should do the titration drop by drop rather than just open the cap and wait for it all to come out

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  10. Here's a site that helps explain what titration actually is.

    http://www.mpcfaculty.net/mark_bishop/titration.htm

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  11. The lab was really confusing. \
    http://www.williams.edu/Chemistry/dbingemann/Chem153/titration.html

    Good site on Tritrations.

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  12. Remember, for the lab the mixture has to be a VERY LIGHT PINK COLOR or you HAVE to restart the whole process over again!

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  13. here is a website on titration
    www.mpcfaculty.net/mark_bishop/titration.htm

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  14. Titration site:

    www2.iq.usp.br/docente/gutz/Curtipot_.html

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  15. http://lrs.ed.uiuc.edu/students/mihyewon/chemlab_experiment.html

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